
 SADABS - Siemens area detector absorption corrections
 ------------------------------------------------------

 Laue group number  1 selected

 Laue group numbers:

 [1] -1                           [8] -3m (rhombohedral axes)
 [2] 2/m (Y unique)               [9] -31m (Z unique)
 [3] mmm                          [10] -3m1 (Z unique)
 [4] 4/m (Z unique)               [11] 6/m (Z unique)
 [5] 4/mmm (Z unique)             [12] 6/mmm (Z unique)
 [6] -3 (rhombohedral axes)       [13] m3
 [7] -3 (Z unique)                [14] m3m

 Friedel opposites treated as equivalent for parameter fitting

 Reading batch  1 from file ka1440.raw
 Reading batch  2 from file ka1441.raw
 Reading batch  3 from file ka1442.raw
 Reading batch  4 from file ka1443.raw
 Reading batch  5 from file ka1444.raw

 Mean and maximum errors in direction cosine check function =   0.001   0.005
 The mean error should not exceed 0.005, and is usually caused by matrix
 changes during data processing.  Maximum 2-theta =   51.65 degrees

   44427 Reflections of which  18424 unique;   20.69 data per frame

 Redundancy:          1     2     3     4     5     6     7     8     9+
 Number of groups:  2404  8818  4606  2414   179     3     0     0     0

 Mean(I/sigma):  -inf    0     1     2     3     5    10    15    20   +inf
 Number of groups:  1506   802   814   707   563  2098  1691  1458  8785


 Settings for parameter refinement:

 (Intensity/sigma) threshold = 5.000
 (Intensity+sigma)/(Mean Intensity) threshold = 0.250
 Savitsky-Golay smoothing applied to incident beam correction
 Maximum odd and even order spherical harmonic coefficients =   1   4

   33938 Reflections employed for parameter determination
 Effective data to parameter ratio =   19.52

 R(int) =   0.0323  before parameter refinement

 Cycle  R(decay)  R(absor)
    1    0.0258    0.0220
    2    0.0202    0.0195
    3    0.0191    0.0188
    4    0.0187    0.0186
    5    0.0186    0.0185
    6    0.0185    0.0185
    7    0.0185    0.0184
    8    0.0184    0.0184
    9    0.0184    0.0184
   10    0.0184    0.0184

 R(int) =   0.0184  after parameter refinement

 Batch  R(int)   Factor range   Sigma(ib) Sigma(db) K(sigI)  Total  I>2sig(I)
    1   0.0198   0.901 -  1.123   0.0263   0.0243    1.062   12464   10342
    2   0.0208   0.907 -  1.125   0.0306   0.0261    1.105    9058    8103
    3   0.0194   0.901 -  1.029   0.0202   0.0190    1.054   12512    9996
    4   0.0214   0.931 -  1.134   0.0305   0.0224    1.127    8929    8059
    5   0.0175   0.954 -  1.124   0.0204   0.0165    0.920    1464    1315

 Sigma(ib) and sigma(db) are the square roots of the variances
 of the normalized incident and diffracted beam correction factors.
 K(sigI) multiplies the sigma(I) values for the batch in question.

 Background contribution to sig(I) = 0.0050 times mean intensity

 2-theta dependent absorption corrections applied for an effective sphere
 with mu*diameter =   0.754

   44427 Corrected reflections written to file ka144.hkl
 Maximum and minimum effective transmission:  0.580324  0.516030

