Single palladium sites supported on carbon capsules : synthesis, structure, and catalysis : a thesis presented in partial fulfilment of the requirements of the degree of Masters of Science in Chemistry at Massey University, Manawatu, New Zealand

Abstract

This work investigates the impregnation of palladium into hollow carbon capsules through a novel synthesis method. This work investigates the feasibility of the method, improves on the method and suggests further improvements. The formation of palladium nanoparticles in hollow carbon capsules is investigated by varying the loading of palladium. This is further investigated by demonstrating the effect of other synthesis variables. The synthesized single palladium sites supported on hollow carbon capsules are then investigated for catalytic activity. These catalysts were found to be catalytically active for the Suzuki coupling reaction.