Controlling Topology of a Telomeric G-quadruplex DNA With a Chemical Cross-link

dc.contributor.authorChilton B
dc.contributor.authorEdwards PJB
dc.contributor.authorJameson GB
dc.contributor.authorHale TK
dc.contributor.authorFilichev VV
dc.date.accessioned2025-07-08T03:22:49Z
dc.date.available2025-07-08T03:22:49Z
dc.date.issued2025-06-18
dc.description.abstractDNA G-quadruplexes (G4s) are noncanonical structures formed in guanine-rich sequences. Within the human genome, they are nonrandomly distributed and influence DNA replication, gene expression, and genome maintenance. Numerous proteins involved in these processes have been identified as G4-binding proteins. However, the interaction of proteins with G4s in the context of double-stranded DNA in vitro has been difficult to study due to the transient nature of G4s in the presence of complementary DNA. To overcome this challenge, introducing internal covalent cross-links between distant nucleotides within the DNA sequence may promote pre-folding of G4 structures, thereby shifting the thermodynamic equilibrium toward G4-formation. We used a Cu(I)-catalyzed azide–alkyne cycloaddition to create a cross-link between 2′-O-propargylguanosine and N<sup>6</sup>-azidoethyl-2′-deoxyadenosine in the DNA telomeric sequence (TAG<inf>3</inf>T)<inf>2</inf>. A cross-link between G3 and A8 reinforced the parallel G4 topology that was stable in the presence of complementary DNA. Moreover, even in the presence of its complementary strand, this cross-linked G4 recruited the parent native DNA (TAG<inf>3</inf>T)<inf>2</inf> to form a hybrid G4. These results suggest that cross-linking provides a useful tool for stabilizing noncanonical DNA structures in the presence of complementary strands, enabling their study within the context of genomic DNA.
dc.identifier.citationChilton B, Edwards PJB, Jameson GB, Hale TK, Filichev VV. (2025). Controlling Topology of a Telomeric G-quadruplex DNA With a Chemical Cross-link. Chemistry A European Journal.
dc.identifier.doi10.1002/chem.202501467
dc.identifier.eissn1521-3765
dc.identifier.elements-typejournal-article
dc.identifier.issn0947-6539
dc.identifier.urihttps://mro.massey.ac.nz/handle/10179/73167
dc.publisherWiley-VCH GmbH, Germany
dc.relation.isPartOfChemistry A European Journal
dc.rights(c) 2025 The Author/s
dc.rightsCC BY 4.0
dc.rights.urihttps://creativecommons.org/licenses/by/4.0/
dc.titleControlling Topology of a Telomeric G-quadruplex DNA With a Chemical Cross-link
dc.typeJournal article
pubs.elements-id501422
pubs.organisational-groupOther
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